p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:1283670-91-6
Molecular Formula:C₂₁H₂₅ClO₁₀
Molecular Weight:472.877
Hs Code.:

Synonyms:p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Technology Process of p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 2 articles about p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 873-76-7
para-Chlorobenzyl alcohol

: 6919-96-6
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1283670-91-6
p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With silver carbonate; In diethyl ether; dichloromethane; at 20 ℃; for 10h; Molecular sieve; Inert atmosphere; Darkness;
DOI:10.1248/cpb.58.1627

Reference yield: 49.0%

: 873-76-7
para-Chlorobenzyl alcohol

: 604-69-3
β-D-glucose pentaacetate

: 1283670-91-6
p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: p-chlorobenzyl 2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; Overall yield = 57 %; Overall yield = 716 mg; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02672