N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide

Base Information

Chemical Name:N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide
CAS No.:1426677-84-0
Molecular Formula:C₂₂H₁₈ClNO₄S
Molecular Weight:427.908
Hs Code.:

Synonyms:N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide

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Chemical Property of N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide

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Technology Process of N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide

There total 4 articles about N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1426678-01-4
C₂₂H₂₀ClNO₄S

: 1426677-84-0
N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/cs4000014

Reference yield:

: 37585-25-4
2-amino-5-chlorobenzyl alcohol

: 1426677-84-0
N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 12 h / 0 °C / Inert atmosphere; Reflux

2: potassium carbonate / acetone / 24 h / 20 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; potassium carbonate; Dess-Martin periodane; In dichloromethane; acetone;
DOI:10.1021/cs4000014

Reference yield:

: 675578-47-9
N-(4-chloro-2-(hydroxymethyl)phenyl)-4-methylbenzenesulfonamide

: 1426677-84-0
N-(4-chloro-2-formylphenyl)-4-methyl-N-(2-oxo-2-phenylethyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 24 h / 20 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With potassium carbonate; Dess-Martin periodane; In dichloromethane; acetone;
DOI:10.1021/cs4000014