C₆₀H₁₀₉NO₁₁Si₃

Base Information

Chemical Name:C₆₀H₁₀₉NO₁₁Si₃
CAS No.:152299-76-8
Molecular Formula:C₆₀H₁₀₉NO₁₁Si₃
Molecular Weight:1104.78
Hs Code.:

C<sub>60</sub>H<sub>109</sub>NO<sub>11</sub>Si<sub>3</sub>

Synonyms:C₆₀H₁₀₉NO₁₁Si₃

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Chemical Property of C₆₀H₁₀₉NO₁₁Si₃

Chemical Property:

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Technology Process of C₆₀H₁₀₉NO₁₁Si₃

There total 24 articles about C₆₀H₁₀₉NO₁₁Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75265-80-4
3-allyl-hex-5-en-2-one

: 152299-76-8
C₆₀H₁₀₉NO₁₁Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N

2: 87 percent / BF₃*OEt₂ / CH₂Cl₂ / -78 °C

3: 85 percent / lutidine, TMSOTf / CH₂Cl₂

4: 81 percent / PyBrop, i-Pr₂NEt

5: 1.) TFA, 2.) DMP, 3.) DDQ, 4.) DMP

With trimethylsilyl trifluoromethanesulfonate; phthalic acid dimethyl ester; lutidine; boron trifluoride diethyl etherate; triethylamine; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1021/ja00075a092

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 152299-76-8
C₆₀H₁₀₉NO₁₁Si₃

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / lutidine, TMSOTf / CH₂Cl₂

2: 81 percent / PyBrop, i-Pr₂NEt

3: 1.) TFA, 2.) DMP, 3.) DDQ, 4.) DMP

With trimethylsilyl trifluoromethanesulfonate; phthalic acid dimethyl ester; lutidine; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1021/ja00075a092

Reference yield:

: 131719-86-3
(R)-3-[(1S,3R,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-3-methoxy-cyclohexyl]-2-methyl-propionaldehyde

: 152299-76-8
C₆₀H₁₀₉NO₁₁Si₃

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / tetrahydrofuran / -78 °C

2: 85 percent / EDCl, DMAP / CH₂Cl₂

3: 78 percent / OsO₄, NMO, Pb(OAc)4

4: 87 percent / BF₃*OEt₂ / CH₂Cl₂ / -78 °C

5: 85 percent / lutidine, TMSOTf / CH₂Cl₂

6: 81 percent / PyBrop, i-Pr₂NEt

7: 1.) TFA, 2.) DMP, 3.) DDQ, 4.) DMP

With lead(IV) acetate; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; trimethylsilyl trifluoromethanesulfonate; phthalic acid dimethyl ester; lutidine; boron trifluoride diethyl etherate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00075a092