1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil

Base Information

Chemical Name:1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil
CAS No.:130745-30-1
Molecular Formula:C₂₆H₃₀N₂O₄Si
Molecular Weight:462.621
Hs Code.:

Synonyms:1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil

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Chemical Property of 1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil

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Technology Process of 1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil

There total 6 articles about 1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 130745-29-8
1-(5-O-tert-butyldiphenylsilyl-2,3-O-diphenoxythiocarbonyl-β-D-arabinofuranosyl)-6-methyluracil

: 130745-30-1
1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil

Guidance literature:: With 2,2'-azobis(2-propionitrile); tri-n-butyl-tin hydride; In toluene; at 100 ℃; for 0.25h;

Reference yield:

: 130745-27-6
2,2'-anhydro-1-(5-O-tert-butyldiphenylsilyl-β-D-arabinofuranosyl)-6-methyluracil

: 130745-30-1
1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide monohydrate / methanol; H₂O / Ambient temperature

2: 67 percent / 4-dimethylaminopyridine / acetonitrile / 20 h / Ambient temperature

3: 80 percent / tributyltin hydride, 2,2'-azobis(2-propionitrile) / toluene / 0.25 h / 100 °C

With dmap; lithium hydroxide; 2,2'-azobis(2-propionitrile); tri-n-butyl-tin hydride; In methanol; water; toluene; acetonitrile;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 130745-30-1
1-(5-O-tert-butyldiphenylsilyl-2,3-didehydro-2,3-dideoxy-β-D-pentofuranosyl)-6-methyluracil

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole / dimethylformamide / Ambient temperature

2: lithium hydroxide monohydrate / methanol; H₂O / Ambient temperature

3: 67 percent / 4-dimethylaminopyridine / acetonitrile / 20 h / Ambient temperature

4: 80 percent / tributyltin hydride, 2,2'-azobis(2-propionitrile) / toluene / 0.25 h / 100 °C

With 1H-imidazole; dmap; lithium hydroxide; 2,2'-azobis(2-propionitrile); tri-n-butyl-tin hydride; In methanol; water; N,N-dimethyl-formamide; toluene; acetonitrile;