trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide

Base Information

Chemical Name:trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide
CAS No.:1594112-91-0
Molecular Formula:C₃₁H₄₅BrNiP₂
Molecular Weight:618.24
Hs Code.:

Synonyms:trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide

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Chemical Property of trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide

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Technology Process of trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide

There total 3 articles about trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 19615-77-1,25456-40-0
trans-Ni(phenyldimethylphosphine)2Br₂

: 108894-99-1
(2,4,6-triisopropylphenyl)magnesium bromide

: 1594112-91-0
trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 0.25h;

Reference yield: 83.0%

: 19615-77-1,25456-40-0
bis(dimethylphenylphosphine)nickel(II) bromide

: 108894-99-1
(2,4,6-triisopropylphenyl)magnesium bromide

: 1594112-91-0
trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 0.25h;
DOI:10.1021/om500156q

Reference yield:

: 672-66-2
Dimethyl(phenyl)phosphine

: 1594112-91-0
trans-bis(dimethylphenylphosphine)(2,4,6-triisopropylphenyl)nickel(II) bromide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 0.5 h / 80 °C / Sealed tube; Inert atmosphere

2: tetrahydrofuran / 0.25 h / 0 °C

In tetrahydrofuran; ethanol;
DOI:10.1021/om500156q