1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol

Base Information

Chemical Name:1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol
CAS No.:177284-84-3
Molecular Formula:C₁₉H₂₈O₈
Molecular Weight:384.427
Hs Code.:

Synonyms:1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol

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Chemical Property of 1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol

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Technology Process of 1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol

There total 4 articles about 1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40983-58-2
methyl shikimate

: 177284-84-3
1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / P₂O₅ / CHCl₃ / 20 h / Ambient temperature

2: 6.47 g / diisobutylaluminum hydride / tetrahydrofuran; hexane

3: 5.1 g / sodium hydride / tetrahydrofuran / 6 h / Heating

4: 1.) BH₃*THF, 2.) H₂O₂, NaOH / 1.) THF, 0 deg C, 1.7 h, 2.) water, heating

With sodium hydroxide; borane-THF; dihydrogen peroxide; phosphorus pentoxide; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; chloroform;
DOI:10.1021/jo952132u

Reference yield:

: 177284-82-1
5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohex-1-enemethanol

: 177284-84-3
1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 5.1 g / sodium hydride / tetrahydrofuran / 6 h / Heating

2: 1.) BH₃*THF, 2.) H₂O₂, NaOH / 1.) THF, 0 deg C, 1.7 h, 2.) water, heating

With sodium hydroxide; borane-THF; dihydrogen peroxide; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo952132u

Reference yield:

: 177284-81-0
methyl 5β-methoxymethoxy-3α,4α-methylenedioxycyclohex-1-enecarboxylate

: 177284-84-3
1α-<<(2,5-dimethoxybenzyl)oxy>methyl>-5β-(methoxymethoxy)-3α,4α-(methylenedioxy)cyclohexan-2β-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 6.47 g / diisobutylaluminum hydride / tetrahydrofuran; hexane

2: 5.1 g / sodium hydride / tetrahydrofuran / 6 h / Heating

3: 1.) BH₃*THF, 2.) H₂O₂, NaOH / 1.) THF, 0 deg C, 1.7 h, 2.) water, heating

With sodium hydroxide; borane-THF; dihydrogen peroxide; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane;
DOI:10.1021/jo952132u