(3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate

Base Information

Chemical Name:(3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate
CAS No.:1376616-32-8
Molecular Formula:C₄₀H₆₁N₃O₉
Molecular Weight:727.939
Hs Code.:

(3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate

Synonyms:(3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate

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Chemical Property of (3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate

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Technology Process of (3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate

There total 4 articles about (3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1236549-06-6
(1S,2S,4S)-4-(2-carbamoyl-2-methylpropyl-carbamoyl)-2-hydroxy-1-{(S)-2-[4-methoxy-3-(3-methoxypropoxy)-benzyl]-3-methylbutyl}-5-methylhexyl-carbamic acid benzyl ester

: 108-24-7
acetic anhydride

: 1376616-32-8
(3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1376616-31-7
C₃₀H₅₁N₃O₅

: 1376616-32-8
(3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 20 °C

2: triethylamine / dichloromethane / 1 h / 20 °C

With triethylamine; In dichloromethane;

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 1376616-32-8
(3S,5S,6S,8S)-8-(4-methoxy-3-(3-methoxypropoxy)benzyl)-3-((3-amino-2,2-dimethyl-3-oxopropyl)carbamoyl)-6-(benzyloxycarbonyl)-2,9-dimethyldecan-5-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 20 °C

2: triethylamine / dichloromethane / 1 h / 20 °C

With triethylamine; In dichloromethane;