dithiomethoxycarbonyl α--benzylmalonic ester

Base Information

Chemical Name:dithiomethoxycarbonyl α--benzylmalonic ester
CAS No.:125503-84-6
Molecular Formula:C₁₅H₁₈O₃S₂
Molecular Weight:310.438
Hs Code.:

dithiomethoxycarbonyl α-<acetonyl-1(H)>-benzylmalonic ester

Synonyms:dithiomethoxycarbonyl α--benzylmalonic ester

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Chemical Property of dithiomethoxycarbonyl α--benzylmalonic ester

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Technology Process of dithiomethoxycarbonyl α--benzylmalonic ester

There total 6 articles about dithiomethoxycarbonyl α--benzylmalonic ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 125503-76-6
2,7-Diaza-1,5-diphenyl-bicyclo<2.2.2>octane-3,8-dithione

: 125503-84-6
dithiomethoxycarbonyl α--benzylmalonic ester

Guidance literature:: With sodium hydroxide; In ethanol; for 2h; Ambient temperature;
DOI:10.1007/BF00482496

Reference yield: 70.0%

: 125503-79-9
2,7-Diaza-1,5-diphenyl-3,8-di(methylthio)bicyclo<2.2.2>octa-2,7-diene

: 125503-84-6
dithiomethoxycarbonyl α--benzylmalonic ester

Guidance literature:: With hydrogenchloride; In ethanol; for 1h;
DOI:10.1007/BF00482496

Reference yield:

: 57162-18-2
2-oxo-4,6-diphenyl-1,2,3,4-tetrahydropyridine-3-carboxamide

: 125503-84-6
dithiomethoxycarbonyl α--benzylmalonic ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / 1N NaOH / ethanol / 1.5 h / Heating

2: 76 percent / Lawesson's reagent / benzene / 3 h / Heating

3: 75 percent / aqueous NaOH / ethanol / 2 h / Ambient temperature

With Lawessons reagent; sodium hydroxide; In ethanol; benzene;
DOI:10.1007/BF00482496