(E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide

Base Information

Chemical Name:(E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide
CAS No.:1132888-64-2
Molecular Formula:C₂₃H₁₉BrN₄O₂S
Molecular Weight:495.399
Hs Code.:

Synonyms:(E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide

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Chemical Property of (E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide

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Technology Process of (E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide

There total 3 articles about (E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 167156-19-6
4-ethynyl-N-methyl-N-phenylbenzenesulfonamide

: 1132789-90-2
(E)-1-azido-4-(2-bromovinyl)benzene

: 1132888-64-2
(E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide

Guidance literature:: With copper(l) iodide; sodium L-ascorbate; In dimethyl sulfoxide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1007/s11172-010-0100-9

Reference yield:

: 133463-51-1
(E)-3-(4-azidophenyl)acrylic acid

: 1132888-64-2
(E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; lithium acetate / water; acetonitrile / 0.17 h / 20 °C

2: copper(l) iodide; sodium L-ascorbate / dimethyl sulfoxide / 12 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; copper(l) iodide; lithium acetate; sodium L-ascorbate; In water; dimethyl sulfoxide; acetonitrile;
DOI:10.1007/s11172-010-0100-9

Reference yield:

: 882-06-4
4-nitro-trans-cinnamic acid

: 1132888-64-2
(E)-4-{1-[4-(2-bromovinyl)phenyl]-1,2,3-triazol-4-yl}-N-methyl-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc / water; acetic acid / 5 h / -20 °C

1.2: 0 °C

2.1: N-Bromosuccinimide; lithium acetate / water; acetonitrile / 0.17 h / 20 °C

3.1: copper(l) iodide; sodium L-ascorbate / dimethyl sulfoxide / 12 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; copper(l) iodide; lithium acetate; sodium L-ascorbate; zinc; In water; acetic acid; dimethyl sulfoxide; acetonitrile;
DOI:10.1007/s11172-010-0100-9