bis(2,6-diisopropylphenyl)dichlorogermane

Base Information

Chemical Name:bis(2,6-diisopropylphenyl)dichlorogermane
CAS No.:125346-76-1
Molecular Formula:C₂₄H₃₄Cl₂Ge
Molecular Weight:466.03
Hs Code.:

Synonyms:bis(2,6-diisopropylphenyl)dichlorogermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2,6-diisopropylphenyl)dichlorogermane

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Technology Process of bis(2,6-diisopropylphenyl)dichlorogermane

There total 1 articles about bis(2,6-diisopropylphenyl)dichlorogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 125346-75-0
bis(2,6-diisopropylphenyl)germane

: 125346-76-1
bis(2,6-diisopropylphenyl)dichlorogermane

Guidance literature:: With tetrachloromethane; dibenzoyl peroxide; In tetrachloromethane; heating to reflux for 3 h, protective gas; concn. on a rotary evaporator, Kugelrohr distn. (110-125°C/0.05 torr);
DOI:10.1016/0022-328X(89)87203-1

Reference yield: 25.0%

: 125346-76-1
bis(2,6-diisopropylphenyl)dichlorogermane

: 861718-25-4
lithium naphthalene

: 91-20-3,71998-51-1,72931-45-4
naphthalene

: 119111-41-0
tetrakis(2,6-diisopropylphenyl)digermene

Guidance literature:: In 1,2-dimethoxyethane; under protective gas, stirring for 2 h at -78°C, warming to 20°C for 4 h; evapn. of solvent and naphthalene, residue is dissolved in toluene, filtered, concd., recrystd.,(toluene, isopropanol);
DOI:10.1016/0022-328X(89)87203-1