C₂₇H₃₄NO₁₀P

Base Information

• Chemical Name: C₂₇H₃₄NO₁₀P
• CAS No.: 1446694-12-7
• Molecular Formula: C₂₇H₃₄NO₁₀P
• Molecular Weight: 563.541
• Mol file: 1446694-12-7.mol

Synonyms:C₂₇H₃₄NO₁₀P

Chemical Property of C₂₇H₃₄NO₁₀P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₇H₃₄NO₁₀P

There total 3 articles about C₂₇H₃₄NO₁₀P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl 2-methylenepentanedioate (5621-44-3) + C22H30NO6PSi → C27H34NO10P (1446694-12-7)

Guidance literature:

at 90 ℃; for 3h;

DOI:10.1016/j.bmcl.2013.05.069

Reference yield:

L-2-<<(benzyloxy)carbonyl>amino>-3-butenoic acid benzyl ester (130096-70-7) → C27H34NO10P (1446694-12-7)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonium hypophosphorous acid; triethyl borane / tetrahydrofuran; methanol / 3 h

2: 1 h / 110 °C / Inert atmosphere

3: 3 h / 90 °C

With ammonium hypophosphorous acid; triethyl borane; In tetrahydrofuran; methanol;

DOI:10.1016/j.bmcl.2013.05.069

Reference yield:

C19H22NO6P → C27H34NO10P (1446694-12-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1 h / 110 °C / Inert atmosphere

2: 3 h / 90 °C

DOI:10.1016/j.bmcl.2013.05.069

upstream raw materials:

L-2-<<(benzyloxy)carbonyl>amino>-3-butenoic acid benzyl ester

dimethyl 2-methylenepentanedioate

Downstream raw materials:

C₂₈H₃₆NO₁₀P