H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1)

Base Information

• Chemical Name: H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1)
• CAS No.: 1092940-40-3
• Molecular Formula: C₆₆H₅₃N₃O₈
• Molecular Weight: 1016.16

Synonyms:H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1)

Chemical Property of H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1)

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Technology Process of H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1)

There total 2 articles about H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

4,7-dihydro-4,7-ethano-2H-isoindole (118824-61-6) + methyl 4-formylbenzoate (1571-08-0) → H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1) (1092940-40-3) + C76H60N4O8Zn

Guidance literature:

4,7-dihydro-4,7-ethano-2H-isoindole; methyl 4-formylbenzoate; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere; Darkness;

With chloranil; In dichloromethane; for 2h;

With zinc diacetate; In methanol; for 12h;

DOI:10.1021/ja8068769

Reference yield:

4,7-dihydro-4,7-ethano-2H-isoindole (118824-61-6) + methyl 4-formylbenzoate (1571-08-0) → H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1) (1092940-40-3) + C76H62N4O8

Guidance literature:

4,7-dihydro-4,7-ethano-2H-isoindole; methyl 4-formylbenzoate; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere; Darkness;

With chloranil; In dichloromethane; for 2h;

DOI:10.1021/ja8068769

Reference yield: 100.0%

H-5,10,11,16-tetra(4-methylbenzoate)[14]tri(bicyclo[2.2.2]octadiene)triphyrin(2.1.1) (1092940-40-3) → H-5,10,11,16-tetra((4-methylbenzoate)phenyl)[14]tribenzotriphyrin(2.1.1) (1092940-38-9)

Guidance literature:

at 220 ℃; for 0.333333h; under 2 Torr;

DOI:10.1021/ja8068769

upstream raw materials:

4,7-dihydro-4,7-ethano-2H-isoindole

methyl 4-formylbenzoate

Downstream raw materials:

H-5,10,11,16-tetra((4-methylbenzoate)phenyl)[14]tribenzotriphyrin(2.1.1)

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