1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose

Base Information

Chemical Name:1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose
CAS No.:78188-24-6
Molecular Formula:C₁₈H₁₈F₃NO₈
Molecular Weight:433.338
Hs Code.:

Synonyms:1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose

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Chemical Property of 1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose

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Technology Process of 1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose

There total 3 articles about 1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 70894-62-1
3-(trifluoroacetamido)-1,2-O-isopropylidene-5-O-benzoyl-3-deoxy-α-D-ribofuranose

: 108-24-7
acetic anhydride

: 78188-24-6
1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose

Guidance literature:: With sulfuric acid; In acetic acid; at 20 ℃; for 15h;

Reference yield:

: 91363-90-5
((3aR,5S,6R,6aR)-6-azido-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl benzoate

: 78188-24-6
1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / 10percent Pd/C / ethanol / 0.75 h / 20 °C

2: 97 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

3: 75 percent / 96percent sulfuric acid / acetic acid / 15 h / 20 °C

With pyridine; sulfuric acid; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid;

Reference yield:

: 91363-91-6
3-amino-5-O-benzoyl-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

: 78188-24-6
1,2-di-O-acetyl-3-deoxy-3-(trifluoroacetamido)-5-O-benzoyl-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

2: 75 percent / 96percent sulfuric acid / acetic acid / 15 h / 20 °C

With pyridine; sulfuric acid; In dichloromethane; acetic acid;