C₂₅H₄₂O₅Si

Base Information

Chemical Name:C₂₅H₄₂O₅Si
CAS No.:1293966-65-0
Molecular Formula:C₂₅H₄₂O₅Si
Molecular Weight:450.691
Hs Code.:

C<sub>25</sub>H<sub>42</sub>O<sub>5</sub>Si

Synonyms:C₂₅H₄₂O₅Si

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Chemical Property of C₂₅H₄₂O₅Si

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Technology Process of C₂₅H₄₂O₅Si

There total 13 articles about C₂₅H₄₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1293966-64-9
C₃₅H₅₁NO₆Si

: 1293966-65-0
C₂₅H₄₂O₅Si

Guidance literature:: With lithium hydroxide monohydrate; water; dihydrogen peroxide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol2007296

Reference yield:

: 1255763-92-8
C₁₆H₂₂O₃

: 1293966-65-0
C₂₅H₄₂O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 15 h / -78 - 20 °C / Inert atmosphere

2: dihydrogen peroxide / methanol; dichloromethane; water / 1 h / 0 °C / Inert atmosphere

3: 2,6-dimethylpyridine / dichloromethane / 3 h / 0 °C / Inert atmosphere

4: lithium hydroxide monohydrate; water; dihydrogen peroxide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; lithium hydroxide monohydrate; water; dihydrogen peroxide; In tetrahydrofuran; methanol; dichloromethane; water; 1: Aldol condensation;
DOI:10.1021/ol2007296

Reference yield:

: 1293966-59-2
C₁₂H₂₈O₂Si

: 1293966-65-0
C₂₅H₄₂O₅Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 3 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -20 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

3.2: 4 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

5.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C / Inert atmosphere

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

6.2: 0 °C / Inert atmosphere

7.1: water; calcium carbonate; methyl iodide / acetonitrile / 24 h / 40 °C / Inert atmosphere

8.1: dichloromethane / 15 h / -78 - 20 °C / Inert atmosphere

9.1: dihydrogen peroxide / methanol; dichloromethane; water / 1 h / 0 °C / Inert atmosphere

10.1: 2,6-dimethylpyridine / dichloromethane / 3 h / 0 °C / Inert atmosphere

11.1: lithium hydroxide monohydrate; water; dihydrogen peroxide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; n-butyllithium; lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; water; dihydrogen peroxide; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; sodium hydride; triethylamine; calcium carbonate; methyl iodide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; mineral oil; 6.2: Wittig reaction / 8.1: Aldol condensation;
DOI:10.1021/ol2007296