Technology Process of C36H39NO7
There total 6 articles about C36H39NO7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C36H37NO7;
With
triethylsilane; phenylborondichloride;
In
dichloromethane;
at -78 ℃;
for 1.5h;
Molecular sieve;
With
methanol; triethylamine;
In
dichloromethane;
at -78 ℃;
DOI:10.1039/c2cc17393j
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrabutylammoniun azide / toluene / 2.5 h / 65 - 100 °C
2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C
2.2: 0 - 20 °C
3.1: water; triphenylphosphine / tetrahydrofuran / 3 h / 45 °C
4.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C
5.1: triethylsilane; phenylborondichloride / dichloromethane / 1.5 h / -78 °C / Molecular sieve
5.2: -78 °C
With
triethylsilane; phenylborondichloride; water; tetrabutylammoniun azide; sodium hydride; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2cc17393j
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridine / dichloromethane / 3 h / -20 - 0 °C
2.1: tetrabutylammoniun azide / toluene / 2.5 h / 65 - 100 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C
3.2: 0 - 20 °C
4.1: water; triphenylphosphine / tetrahydrofuran / 3 h / 45 °C
5.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C
6.1: triethylsilane; phenylborondichloride / dichloromethane / 1.5 h / -78 °C / Molecular sieve
6.2: -78 °C
With
pyridine; triethylsilane; phenylborondichloride; water; tetrabutylammoniun azide; sodium hydride; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c2cc17393j