{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-4-{[2-(hydroxymethyl)phenyl]dimethylsilyl}benzene

Base Information

Chemical Name:{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-4-{[2-(hydroxymethyl)phenyl]dimethylsilyl}benzene
CAS No.:1239354-32-5
Molecular Formula:C₂₉H₃₈O₃Si₂
Molecular Weight:490.79
Hs Code.:

Synonyms:{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-4-{[2-(hydroxymethyl)phenyl]dimethylsilyl}benzene

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Chemical Property of {dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-4-{[2-(hydroxymethyl)phenyl]dimethylsilyl}benzene

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Technology Process of {dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-4-{[2-(hydroxymethyl)phenyl]dimethylsilyl}benzene

There total 1 articles about {dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-4-{[2-(hydroxymethyl)phenyl]dimethylsilyl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 953412-90-3
C₂₀H₂₅BrO₂Si

: 321903-29-1
1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole

: 1239354-32-5
{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-4-{[2-(hydroxymethyl)phenyl]dimethylsilyl}benzene

Guidance literature:: C₂₀H₂₅BrO₂Si; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

1,1-dimethyl-1,3-dihydrobenzo[c][1,2]oxasilole; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1246/bcsj.20090325

Reference yield: 87.0%

: 953412-93-6
[2-(acetoxymethyl)phenyl](2-bromo-5-thienyl)dimethylsilane

: 1239354-32-5
{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}-4-{[2-(hydroxymethyl)phenyl]dimethylsilyl}benzene

: 1239354-37-0
2-{[2-(acetoxymethyl)phenyl]dimethylsilyl}-5-(4-{dimethyl[2-(tetrahydro-2H-pyranyloxymethyl)phenyl]silyl}phenyl)thiophene

Guidance literature:: With copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); potassium carbonate; ruphos; In tetrahydrofuran; N,N-dimethyl-formamide; at 75 ℃; for 8h; Inert atmosphere;
DOI:10.1246/bcsj.20090325