Technology Process of C9H17NO3*ClH
There total 7 articles about C9H17NO3*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
8-methoxymethyl-1,3-diaza-spiro[4.5]decane-2,4-dione;
With
water; potassium hydroxide;
Heating;
Reflux;
Inert atmosphere;
With
hydrogenchloride; water;
at 0 - 10 ℃;
pH=4 - 5;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: hydrogen / Ru/Al2O3 / methanol / 120 °C / 90009 Torr
2.1: amberlyst-15 / dichloromethane / 2 h
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C
3.2: 0 °C
4.1: sodium hydride / tetrahydrofuran / 20 - 60 °C
4.2: 20 °C
5.1: toluene-4-sulfonic acid / methanol / 20 °C
6.1: sodium hypochlorite; acetic acid / 15 °C
7.1: sodium cyanide / water / 20 - 60 °C
8.1: water; potassium hydroxide / Heating; Reflux; Inert atmosphere
8.2: 0 - 10 °C / pH 4 - 5
With
sodium hypochlorite; lithium aluminium tetrahydride; amberlyst-15; sodium cyanide; water; hydrogen; sodium hydride; toluene-4-sulfonic acid; acetic acid; potassium hydroxide;
Ru/Al2O3;
In
tetrahydrofuran; methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / methanol / 20 °C
2.1: sodium hypochlorite; acetic acid / 15 °C
3.1: sodium cyanide / water / 20 - 60 °C
4.1: water; potassium hydroxide / Heating; Reflux; Inert atmosphere
4.2: 0 - 10 °C / pH 4 - 5
With
sodium hypochlorite; sodium cyanide; water; toluene-4-sulfonic acid; acetic acid; potassium hydroxide;
In
methanol; water;