(E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

Base Information

Chemical Name:(E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene
CAS No.:103628-15-5
Molecular Formula:C₃₁H₂₂ClF₇O₂
Molecular Weight:594.956
Hs Code.:

Synonyms:(E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

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Chemical Property of (E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

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Technology Process of (E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

There total 7 articles about (E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 129942-65-0
C₁₃H₄ClF₇OZn

: 129920-99-6
(E)-1-bromo-1-<4-(2-chloroethoxy)phenyl>-2-phenyl-1-butene

: 103628-14-4
(Z)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

: 103628-15-5
(E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 1h; Yield given;
DOI:10.1021/jo00312a027

Reference yield:

: 103628-22-4
1--2-phenyl-butan-1-one

: 103628-15-5
(E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg, BrCH₂CH₂Br / 1.) ether, 20 deg C, 1 h, 2.) 20 h, r.t.

2: conc. HCl / 4 h / Heating

With hydrogenchloride; magnesium; ethylene dibromide;

Reference yield:

: 129942-66-1
C₁₃H₄ClF₇MgO

: 129920-99-6
(E)-1-bromo-1-<4-(2-chloroethoxy)phenyl>-2-phenyl-1-butene

: 103628-14-4
(Z)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

: 103628-15-5
(E)-1-<4-(2-chloroethoxy)phenyl>-1-<4-<2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenoxy>phenyl>-2-phenyl-1-butene

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1021/jo00312a027