2-amino-N-(1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-benzenesulfonamide hydrochloride

Base Information

Chemical Name:2-amino-N-(1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-benzenesulfonamide hydrochloride
CAS No.:1196112-01-2
Molecular Formula:C₁₃H₁₃BN₂O₄S
Molecular Weight:304.134
Hs Code.:

Synonyms:2-amino-N-(1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-benzenesulfonamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-N-(1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-benzenesulfonamide hydrochloride

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Technology Process of 2-amino-N-(1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-benzenesulfonamide hydrochloride

There total 2 articles about 2-amino-N-(1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-benzenesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1196112-00-1
PT₆₅₉

: 1196112-01-2
2-amino-N-(1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-benzenesulfonamide hydrochloride

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 2.5h; under 2585.81 Torr;

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 117098-94-9
(5-amino-2-hydroxymethylphenyl)boronic acid

: 1196112-01-2
2-amino-N-(1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-benzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 4-methyl-morpholine / acetonitrile / 20 °C

2: hydrogen / palladium 10% on activated carbon / ethanol / 2.5 h / 20 °C / 2585.81 Torr

With 4-methyl-morpholine; hydrogen; palladium 10% on activated carbon; In ethanol; acetonitrile;