Technology Process of C29H28N2O6
There total 12 articles about C29H28N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at -5 ℃;
for 6h;
DOI:10.1021/ja500548e
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1H-imidazole; sodium hydride / tetrahydrofuran; mineral oil / 0 - 25 °C
1.2: 1 h / 0 - 25 °C
1.3: 1 h / 0 - 25 °C
2.1: toluene / 36 h / 150 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
3.2: 2.5 h / -78 °C
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 - 25 °C
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / -5 °C
With
1H-imidazole; tetrabutyl ammonium fluoride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1021/ja500548e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 2.5 h / -78 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 - 25 °C
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / -5 °C
With
tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja500548e