2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine

Base Information

Chemical Name:2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine
CAS No.:1431328-84-5
Molecular Formula:C₃₁H₅₇NO₄Si
Molecular Weight:535.883
Hs Code.:

Synonyms:2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine

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Chemical Property of 2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine

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Technology Process of 2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine

There total 4 articles about 2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 998-30-1
Triethoxysilane

: 1431328-83-4
2,2,6,6-tetramethyl-1-(1-(4-(oct-7-ene-1-yl)phenyl)ethoxy)piperidine

: 1431328-84-5
2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In dichloromethane; at 40 ℃; for 6h;
DOI:10.1002/chem.201200499

Reference yield:

: 159755-11-0
1-bromo-4-(1-bromoethyl)benzene

: 1431328-84-5
2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper; copper(II) bis(trifluoromethanesulfonate); 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 12 h / 75 °C

2.1: 9-borabicyclo[3.3.1]nonane dimer / tetrahydrofuran / 3 h / 0 - 20 °C

2.2: Pd(dppf) / 6 h / 70 °C

3.1: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / dichloromethane / 6 h / 40 °C

With 9-borabicyclo[3.3.1]nonane dimer; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; copper(II) bis(trifluoromethanesulfonate); copper; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1002/chem.201200499

Reference yield:

: 178625-97-3
1-[1-(4-bromophenyl)ethoxy]-2,2,6,6-tetramethylpiperidine

: 1431328-84-5
2,2,6,6-tetramethyl-1-(1-(4-(8-(triethoxysilyl)octyl)phenyl)ethoxy)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 9-borabicyclo[3.3.1]nonane dimer / tetrahydrofuran / 3 h / 0 - 20 °C

1.2: Pd(dppf) / 6 h / 70 °C

2.1: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / dichloromethane / 6 h / 40 °C

With 9-borabicyclo[3.3.1]nonane dimer; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201200499