N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Chemical Name:N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside
CAS No.:1400594-91-3
Molecular Formula:C₉₅H₉₇Cl₃N₈O₁₉
Molecular Weight:1761.22
Hs Code.:

N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Synonyms:N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Chemical Property of N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Technology Process of N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

There total 1 articles about N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1400594-81-1
N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

: 1400594-91-3
N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Guidance literature:: With methanol; hydrazinium monoacetate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ja3069962

Reference yield: 66.0%

: 1400594-91-3
N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

: C₃₅H₃₄Cl₃NO₆

: 1400594-92-4
N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-[O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1→3)]-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; dichloromethane; at -55 - 0 ℃; for 1.5h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja3069962