tert-butyl 2-[(4-methoxybenzyloxy)methyl]-5-tosylpyridine-1(2H)-carboxylate

Base Information

• Chemical Name: tert-butyl 2-[(4-methoxybenzyloxy)methyl]-5-tosylpyridine-1(2H)-carboxylate
• CAS No.: 1190765-56-0
• Molecular Formula: C₂₆H₃₁NO₆S
• Molecular Weight: 485.601

Synonyms:tert-butyl 2-[(4-methoxybenzyloxy)methyl]-5-tosylpyridine-1(2H)-carboxylate

Chemical Property of tert-butyl 2-[(4-methoxybenzyloxy)methyl]-5-tosylpyridine-1(2H)-carboxylate

Chemical Property:

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Technology Process of tert-butyl 2-[(4-methoxybenzyloxy)methyl]-5-tosylpyridine-1(2H)-carboxylate

There total 1 articles about tert-butyl 2-[(4-methoxybenzyloxy)methyl]-5-tosylpyridine-1(2H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

C28H33NO7S3 → tert-butyl 2-[(4-methoxybenzyloxy)methyl]-5-tosylpyridine-1(2H)-carboxylate (1190765-56-0)

Guidance literature:

C₂₈H₃₃NO₇S₃; With 2,2'-azobis(isobutyronitrile); In toluene; Reflux; Inert atmosphere;

With tri-n-butyl-tin hydride; In toluene; for 2h; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2009.07.022

Reference yield: 24.0%

tert-butyl 2-[(4-methoxybenzyloxy)methyl]-5-tosylpyridine-1(2H)-carboxylate (1190765-56-0) → C18H23NO5S (1190765-57-1)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.tet.2009.07.022

Downstream raw materials:

C₁₈H₂₃NO₅S

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