1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde

Base Information

• Chemical Name: 1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde
• CAS No.: 124750-54-5
• Molecular Formula: C₂₆H₃₀N₂O₃
• Molecular Weight: 418.536

Synonyms:1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde

Chemical Property of 1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde

Chemical Property:

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Technology Process of 1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde

There total 14 articles about 1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4(5)-methyl-2-propylimidazole-5(4)-carboxaldehyde + 4'-bromomethyl-biphenyl-2-carboxylic acid tert-butyl ester (114772-40-6) → 1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde (124750-54-5)

Guidance literature:

With potassium carbonate; In N-methyl-acetamide;

Reference yield:

4(5)-methyl-4-proylimidazole-5(4)-carboxaldehyde + 4'-bromomethyl-biphenyl-2-carboxylic acid tert-butyl ester (114772-40-6) → 1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde (124750-54-5)

Guidance literature:

With potassium carbonate; In N-methyl-acetamide;

Reference yield:

4'-bromomethyl-biphenyl-2-carboxylic acid tert-butyl ester (114772-40-6) + 4(5)-methyl-2-propylimidazole-5(4)-carboxaldehyde (68282-59-7) → 1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-4-methyl-2-propylimidazole-5-carboxaldehyde (124750-54-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 24h;

DOI:10.1021/jm00112a031

upstream raw materials:

4'-bromomethyl-biphenyl-2-carboxylic acid tert-butyl ester

4⁽⁵⁾-methyl-2-propylimidazole-5⁽⁴⁾-carboxaldehyde

2-(2-methoxyphenyl)-4,4-dimethyl-2-oxazoline

o-tolylbenzoic acid

Downstream raw materials:

1-<(2'-carboxylbiphenyl-4-yl)methyl>-5-(hydroxymethyl)-4-methyl-2-propylimidazole hydrochloride

1-<<2'-(tert-butoxycarbonyl)biphenyl-4-yl>methyl>-5-(hydroxymethyl)-4-methyl-2-propylimidazole

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