N-Phenyl-N'-(3-methoxy-4-hydroxy-α-amino)benzylhydrazine

Base Information

• Chemical Name: N-Phenyl-N'-(3-methoxy-4-hydroxy-α-amino)benzylhydrazine
• CAS No.: 81323-36-6
• Molecular Formula: C₁₄H₁₇N₃O₂
• Molecular Weight: 259.308
• Mol file: 81323-36-6.mol

Synonyms:N-Phenyl-N'-(3-methoxy-4-hydroxy-α-amino)benzylhydrazine

Chemical Property of N-Phenyl-N'-(3-methoxy-4-hydroxy-α-amino)benzylhydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Phenyl-N'-(3-methoxy-4-hydroxy-α-amino)benzylhydrazine

There total 2 articles about N-Phenyl-N'-(3-methoxy-4-hydroxy-α-amino)benzylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

N-Phenyl-N'-(4-hydroxy-3-methoxy-α-hydroxylamino)benzylhydrazine (81323-18-4) → N-Phenyl-N'-(3-methoxy-4-hydroxy-α-amino)benzylhydrazine (81323-36-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In benzene; for 2h; under 930.9 Torr;

Reference yield:

vanilline phenylhydrazone (16435-04-4) → N-Phenyl-N'-(3-methoxy-4-hydroxy-α-amino)benzylhydrazine (81323-36-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / NH₂OH*HCl, NaOAc / ethanol / 2.5 h / Heating

2: 69 percent / H₂ / 5percent Pd/C / benzene / 2 h / 930.9 Torr

With hydroxylamine hydrochloride; hydrogen; sodium acetate; palladium on activated charcoal; In ethanol; benzene;

upstream raw materials:

N-Phenyl-N'-(4-hydroxy-3-methoxy-α-hydroxylamino)benzylhydrazine

vanilline phenylhydrazone

Refernces