C₂₈H₄₈O₆Si

Base Information

Chemical Name:C₂₈H₄₈O₆Si
CAS No.:1209386-19-5
Molecular Formula:C₂₈H₄₈O₆Si
Molecular Weight:508.771
Hs Code.:

C<sub>28</sub>H<sub>48</sub>O<sub>6</sub>Si

Synonyms:C₂₈H₄₈O₆Si

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Chemical Property of C₂₈H₄₈O₆Si

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Technology Process of C₂₈H₄₈O₆Si

There total 15 articles about C₂₈H₄₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1209386-18-4
C₂₇H₄₆O₆Si

: 1209386-19-5
C₂₈H₄₈O₆Si

Guidance literature:: C₂₇H₄₆O₆Si; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.333333h; Inert atmosphere;

With dimethyl sulfate; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo400260m

Reference yield:

: C₃₄H₅₂O₇Si

: 1209386-19-5
C₂₈H₄₈O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl ether / 0 °C / Inert atmosphere

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.77 h / 0 °C / pH 7 / Inert atmosphere

3.1: camphor-10-sulfonic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C / Inert atmosphere

4.2: 1.5 h / 0 - 20 °C / Inert atmosphere

With camphor-10-sulfonic acid; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; mineral oil;
DOI:10.1021/jo400260m

Reference yield:

: C₁₉H₂₈O₄

: 1209386-19-5
C₂₈H₄₈O₆Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 0.5 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane; hexane / 0.08 h / -78 °C / Inert atmosphere

3.1: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / -20 °C / Inert atmosphere; Molecular sieve

4.1: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

5.1: dichloromethane / 0.02 h / 0 °C / Inert atmosphere

6.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tributylphosphine; formic acid; triethylamine / 1,4-dioxane / 9.5 h / 20 °C / Inert atmosphere

7.1: 2,6-dimethylpyridine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

8.1: diisobutylaluminium hydride / dichloromethane; hexane / 0.12 h / -78 °C / Inert atmosphere

9.1: D-(-)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / 4 h / -20 °C / Inert atmosphere; Molecular sieve

10.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; sodium chlorite / acetonitrile / 1.5 h / pH 7 / Inert atmosphere

11.1: diethyl ether / 0 °C / Inert atmosphere

12.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.77 h / 0 °C / pH 7 / Inert atmosphere

13.1: camphor-10-sulfonic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

14.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C / Inert atmosphere

14.2: 1.5 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium hypochlorite; sodium chlorite; formic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; L-(+)-diisopropyl tartrate; tributylphosphine; trifluorormethanesulfonic acid; camphor-10-sulfonic acid; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; D-(-)-diisopropyl tartrate; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; diethyl ether; decane; hexane; dichloromethane; cyclohexane; acetonitrile; mineral oil; 3.1: |Sharpless Asymmetric Epoxidation / 4.1: |Parikh-Doering Oxidation / 5.1: |Horner-Wadsworth-Emmons Olefination / 9.1: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/jo400260m