(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester

Base Information

Chemical Name:(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester
CAS No.:97592-10-4
Molecular Formula:C₁₈H₂₃ClO₄
Molecular Weight:338.831
Hs Code.:

Synonyms:(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester

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Chemical Property of (Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester

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Technology Process of (Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester

There total 4 articles about (Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 87102-06-5
6-<(2,4,6-trimethylbenzoyl)oxy>-3-hydroxy-2-methylenehexanoic acid, methyl ester

: 97592-10-4
(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester

Guidance literature:: With N-chloro-succinimide; dimethylsulfide; In dichloromethane; for 12h;
DOI:10.1021/jo00220a034

Reference yield:

: 87102-03-2
3-formylpropyl 2,4,6-trimethyl benzoate

: 97592-10-4
(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / DABCO / 168 h / Ambient temperature

2: 89 percent / N-chlorosuccinimide, Me₂S / CH₂Cl₂ / 12 h

With 1,4-diaza-bicyclo[2.2.2]octane; N-chloro-succinimide; dimethylsulfide; In dichloromethane;
DOI:10.1021/jo00220a034

Reference yield:

: 97592-16-0
4-hydroxybutyl 2,4,6-trimethylbenzoate

: 97592-10-4
(Z)-6-<(2,4,6-trimethylbenzoyl)oxy>-2-(chloromethyl)-2-hexenoic acid, methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / pyridine chlorochromate / CH₂Cl₂ / 2 h

2: 87 percent / DABCO / 168 h / Ambient temperature

3: 89 percent / N-chlorosuccinimide, Me₂S / CH₂Cl₂ / 12 h

With 1,4-diaza-bicyclo[2.2.2]octane; N-chloro-succinimide; dimethylsulfide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/jo00220a034