(Benzylimido)diphosphoric acid tribenzyl ester

Base Information

• Chemical Name: (Benzylimido)diphosphoric acid tribenzyl ester
• CAS No.: 163779-53-1
• Molecular Formula: C₂₈H₂₉NO₆P₂
• Molecular Weight: 537.489

Synonyms:(Benzylimido)diphosphoric acid tribenzyl ester

Chemical Property of (Benzylimido)diphosphoric acid tribenzyl ester

Chemical Property:

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Technology Process of (Benzylimido)diphosphoric acid tribenzyl ester

There total 1 articles about (Benzylimido)diphosphoric acid tribenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C35H35NO6P2 → (Benzylimido)diphosphoric acid tribenzyl ester (163779-53-1)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; for 0.5h; Heating;

DOI:10.1021/jo00114a059

Reference yield: 75.0%

(Benzylimido)diphosphoric acid tribenzyl ester (163779-53-1) + 1-benzyl-2-N-(N',N'-dibenzylformamidine)-9-(2',3'-O-benzylidene-β-D-ribofuranosyl)guanine → 1-benzyl-2-N-(N',N'-dibenzylformamidine)-9-<2',3'-O-benzylidene-5'-O--β-D-ribofuranosyl>guanine

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 60 ℃; for 2h;

DOI:10.1021/jo9806207

Reference yield: 68.0%

(Benzylimido)diphosphoric acid tribenzyl ester (163779-53-1) + 1-benzyl-2-N-(N',N'-dibenzylformamidine)-9-(2'-O-benzyl-β-D-ribofuranosyl)guanine → 1-benzyl-2-N-(N',N'-dibenzylformamidine)-9-<2'-O-benzyl-5'-O--β-D-ribofuranosyl>guanine

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 60 ℃; for 2h;

DOI:10.1021/jo9806207

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