3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate

Base Information

Chemical Name:3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate
CAS No.:3396-72-3
Molecular Formula:C₁₅H₂₀O₆S
Molecular Weight:328.386
Hs Code.:

Synonyms:3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate

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Technology Process of 3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate

There total 11 articles about 3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3396-71-2
3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

: 98-59-9
p-toluenesulfonyl chloride

: 3396-72-3
3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate

Guidance literature:: In pyridine; Ambient temperature;
DOI:10.1016/S0040-4039(99)00877-1

Reference yield:

: 20031-21-4
1,2-O-isopropylidene-α-D-xylose

: 3396-72-3
3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: NaOH

3: n-Bu₃SnH; AIBN

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In pyridine;

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-xylofuranose

: 3396-72-3
3-deoxy-1,2-O-(1-methylethylidene)-α-D-erythro-pentofuranose 4-methylbenzenesufonate

Guidance literature:: Multi-step reaction with 6 steps

1: H₂SO₄ / Ambient temperature

2: 0.2percent HCl / Ambient temperature

3: pyridine / -10 °C

4: 1,1'-thiocarbonyldiimidazole / 1,2-dichloro-ethane / Heating

5: NaOCH₃ / methanol / Ambient temperature

6: pyridine / 0 °C

With pyridine; hydrogenchloride; sulfuric acid; sodium methylate; 1,1'-Thiocarbonyldiimidazole; In methanol; 1,2-dichloro-ethane;