p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:84564-26-1
Molecular Formula:C₅₀H₄₅F₃N₂O₁₆
Molecular Weight:986.906
Hs Code.:

Synonyms:p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 7 articles about p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 84564-25-0
p-trifluoroacetamidophenyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 84564-26-1
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid;
DOI:10.1016/0008-6215(82)85025-8

Reference yield:

: 84564-21-6
p-nitrophenyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

: 84564-26-1
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 41 percent / BaCO₃, Ba(OH)2 * 8 H₂O / dimethylformamide / 2 h

2: 57 percent / silver trifluoromethanesulfonate, 2,4,6-trimethylpyridine / toluene; nitromethane / Ambient temperature

3: H₂ / Adams's catalyst / ethyl acetate

4: pyridine / ethyl acetate / 0.5 h / 60 °C

5: 66 percent / H₂ / 10percent Pd-C / acetic acid

With pyridine; 2,4,6-trimethyl-pyridine; barium dihydroxide; hydrogen; silver trifluoromethanesulfonate; barium carbonate; platinum(IV) oxide; palladium on activated charcoal; In nitromethane; acetic acid; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0008-6215(82)85025-8

Reference yield:

: 84564-22-7
p-nitrophenyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 84564-26-1
p-trifluoroacetamidophenyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / silver trifluoromethanesulfonate, 2,4,6-trimethylpyridine / toluene; nitromethane / Ambient temperature

2: H₂ / Adams's catalyst / ethyl acetate

3: pyridine / ethyl acetate / 0.5 h / 60 °C

4: 66 percent / H₂ / 10percent Pd-C / acetic acid

With pyridine; 2,4,6-trimethyl-pyridine; hydrogen; silver trifluoromethanesulfonate; platinum(IV) oxide; palladium on activated charcoal; In nitromethane; acetic acid; ethyl acetate; toluene;
DOI:10.1016/0008-6215(82)85025-8