(S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester

Base Information

• Chemical Name: (S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester
• CAS No.: 269396-27-2
• Molecular Formula: C₃₉H₄₅N₃O₅
• Molecular Weight: 635.803

Synonyms:(S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester

Chemical Property of (S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester

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Technology Process of (S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester

There total 1 articles about (S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Leu-Phe-OBzl (70637-27-3) + 2-(R,S)-benzyl-3-benzyloxyamino-propionic acid (96866-14-7) → (S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester (269396-27-2)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

DOI:10.1016/S0960-894X(99)00671-X

Reference yield: 80.0%

acetic anhydride (108-24-7) + (S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester (269396-27-2) → (S)-2-{(S)-2-[3-(Acetyl-benzyloxy-amino)-2-benzyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester (269396-35-2)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1016/S0960-894X(99)00671-X

Reference yield: 68.0%

trimethylsilyl isocyanate (1118-02-1) + (S)-2-{(S)-2-[2-(Benzyloxyamino-methyl)-3-phenyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester (269396-27-2) → C40H46N4O6 (269396-36-3)

Guidance literature:

In tetrahydrofuran; Heating;

DOI:10.1016/S0960-894X(99)00671-X

upstream raw materials:

Leu-Phe-OBzl

2-(R,S)-benzyl-3-benzyloxyamino-propionic acid

Downstream raw materials:

C₄₀H₄₆N₄O₆

(S)-2-{(S)-2-[3-(Acetyl-benzyloxy-amino)-2-benzyl-propionylamino]-4-methyl-pentanoylamino}-3-phenyl-propionic acid benzyl ester

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