C₃₅H₅₆O₇S

Base Information

Chemical Name:C₃₅H₅₆O₇S
CAS No.:1355239-52-9
Molecular Formula:C₃₅H₅₆O₇S
Molecular Weight:620.891
Hs Code.:

C<sub>35</sub>H<sub>56</sub>O<sub>7</sub>S

Synonyms:C₃₅H₅₆O₇S

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Chemical Property of C₃₅H₅₆O₇S

Chemical Property:

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Technology Process of C₃₅H₅₆O₇S

There total 1 articles about C₃₅H₅₆O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2432-42-0
S-ethyl propanethioate

: 1119753-98-8
C₃₀H₄₆O₆

: 1355239-52-9
C₃₅H₅₆O₇S

Guidance literature:: S-ethyl propanethioate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

C₃₀H₄₆O₆; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; hexane; water; at -78 ℃; Inert atmosphere;
DOI:10.1021/ol203342e

Reference yield:

: 1355239-52-9
C₃₅H₅₆O₇S

: C₃₃H₅₀O₆

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 2.08 h / 0 - 25 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 0.33 h / 20 - 25 °C / Inert atmosphere

3: quinoline; triethylsilane; 1-hexene / dichloromethane / 8 h / 20 - 25 °C / Inert atmosphere

With pyridine; quinoline; triethylsilane; 1-hexene; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; toluene;
DOI:10.1021/ol203342e

Reference yield:

: 1355239-52-9
C₃₅H₅₆O₇S

: C₆₇H₁₀₈O₁₁Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: pyridine / dichloromethane / 2.08 h / 0 - 25 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 0.33 h / 20 - 25 °C / Inert atmosphere

3.1: quinoline; triethylsilane; 1-hexene / dichloromethane / 8 h / 20 - 25 °C / Inert atmosphere

4.1: diethyl ether / 2 h / -78 - 25 °C / Inert atmosphere

4.2: 1 h / Inert atmosphere; Reflux

5.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 0.17 h / -78 °C / Inert atmosphere

5.2: 1.5 h / -78 - -20 °C / Inert atmosphere

6.1: N-iodo-succinimide / 1,1,1,3',3',3'-hexafluoro-propanol / 0 °C / Inert atmosphere

7.1: water; potassium carbonate / methanol / 7.5 h / 20 - 25 °C / Inert atmosphere

8.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -10 °C / Inert atmosphere

8.2: 1.5 h / -10 - 25 °C / Inert atmosphere

8.3: 20 - 25 °C / Inert atmosphere

9.1: pyridinium p-toluenesulfonate / dichloromethane / 1 h / 20 - 25 °C / Inert atmosphere

10.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

10.2: -78 - 0 °C / Inert atmosphere

11.1: tert.-butyl lithium / diethyl ether; pentane / 1.17 h / -78 °C / Inert atmosphere

11.2: 1.03 h / -78 - 0 °C / Inert atmosphere

11.3: Inert atmosphere

With pyridine; quinoline; triethylsilane; N-iodo-succinimide; n-butyllithium; 1-hexene; oxalyl dichloride; water; tert.-butyl lithium; pyridinium p-toluenesulfonate; potassium carbonate; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; 1,1,1,3',3',3'-hexafluoro-propanol; toluene; pentane; 4.1: Soderquist allylation / 10.1: Swern oxidation / 10.2: Swern oxidation;
DOI:10.1021/ol203342e