2--1-(ethanoyloxy)-1-phenyl-1-propene

Base Information

• Chemical Name: 2--1-(ethanoyloxy)-1-phenyl-1-propene
• CAS No.: 141170-69-6
• Molecular Formula: C₁₇H₂₉NO₂Si₂
• Molecular Weight: 335.594
• Mol file: 141170-69-6.mol

Synonyms:2--1-(ethanoyloxy)-1-phenyl-1-propene

Chemical Property of 2--1-(ethanoyloxy)-1-phenyl-1-propene

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2--1-(ethanoyloxy)-1-phenyl-1-propene

There total 1 articles about 2--1-(ethanoyloxy)-1-phenyl-1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyllithium (917-54-4) + acetic anhydride (108-24-7) + 2-Phenyl-2-(trimethylsilyl)-2-<(trimethylsilyl)oxy>ethanenitrile (138754-40-2) → 2--1-(ethanoyloxy)-1-phenyl-1-propene (141170-69-6)

Guidance literature:

Yield given. Multistep reaction; 1) ether, 25 deg C, overnight, 2) 0 to 25 deg C, 2-3 h;

DOI:10.1021/jo00038a020

Reference yield:

2--1-(ethanoyloxy)-1-phenyl-1-propene (141170-69-6) → 2,4-dimethyl-5-phenyloxazole (23012-31-9)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In chloroform; at 25 ℃; for 96h; Yield given;

DOI:10.1021/jo00038a020

upstream raw materials:

methyllithium

acetic anhydride

2-Phenyl-2-(trimethylsilyl)-2-<(trimethylsilyl)oxy>ethanenitrile

Downstream raw materials:

2,4-dimethyl-5-phenyloxazole