N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide

Base Information

Chemical Name:N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide
CAS No.:1445720-40-0
Molecular Formula:C₁₆H₂₀BrNO₂S₂
Molecular Weight:402.376
Hs Code.:

Synonyms:N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide

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Chemical Property of N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide

Chemical Property:

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Technology Process of N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide

There total 3 articles about N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 78-77-3
Isobutyl bromide

: 1445720-39-7
N-((5-bromothiophen-2-yl)methyl)-1-phenylmethanesulfonamide

: 1445720-40-0
N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide

Guidance literature:: N-((5-bromothiophen-2-yl)methyl)-1-phenylmethanesulfonamide; With sodium hydride; In N,N-dimethyl acetamide; mineral oil; for 0.5h; Inert atmosphere;

Isobutyl bromide; In N,N-dimethyl acetamide; mineral oil; at 20 ℃; for 16h;

Reference yield:

: 1001414-56-7
(5-bromo-2-thienyl)methanamine hydrochloride

: 1445720-40-0
N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

2.1: sodium hydride / N,N-dimethyl acetamide; mineral oil / 0.5 h / Inert atmosphere

2.2: 16 h / 20 °C

With sodium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl acetamide; mineral oil;

Reference yield:

: 1939-99-7
benzenesulfonyl chloride

: 1445720-40-0
N-((5-bromothiophen-2-yl)methyl)-N-isobutyl-1-phenylmethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

2.1: sodium hydride / N,N-dimethyl acetamide; mineral oil / 0.5 h / Inert atmosphere

2.2: 16 h / 20 °C

With sodium hydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl acetamide; mineral oil;