methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate

Base Information

Chemical Name:methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate
CAS No.:1549770-76-4
Molecular Formula:C₂₂H₂₄O₈
Molecular Weight:416.428
Hs Code.:

Synonyms:methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate

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Chemical Property of methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate

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Technology Process of methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate

There total 1 articles about methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 53762-69-9
5-(2-iodoethyl)-3,4-methylenedioxybenzene

: 3807-19-0
methyl 3,4-dimethoxy-2-(methoxycarbonyl)benzeneacetate

: 1549770-76-4
methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate

Guidance literature:: methyl 3,4-dimethoxy-2-(methoxycarbonyl)benzeneacetate; With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; diisopropylamine; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

5-(2-iodoethyl)-3,4-methylenedioxybenzene; In tetrahydrofuran; at 25 ℃; for 7h; Inert atmosphere;
DOI:10.1039/c3ra45312j

Reference yield: 91.0%

: 1549770-76-4
methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate

: 1549771-10-9
4-(benzo[d][1,3]dioxol-5-yl)-2-(3,4-dimethoxy-2-(methoxycarbonyl)phenyl)butanoic acid

Guidance literature:: methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate; With potassium hydroxide; In methanol; water; at 0 - 25 ℃; for 24h;

With hydrogenchloride; In methanol; water; regioselective reaction;
DOI:10.1039/c3ra45312j

Reference yield:

: 1549770-76-4
methyl 6-(4-(benzo[d][1,3]dioxol-5-yl)-1-methoxy-1-oxobutan-2-yl)-2,3-dimethoxybenzoate

: 1549771-30-3
C₂₁H₂₀O₇

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / methanol; water / 24 h / 0 - 25 °C

2: trifluoroacetic anhydride / 3 h / -50 - 25 °C / Inert atmosphere

With trifluoroacetic anhydride; potassium hydroxide; In methanol; water;
DOI:10.1039/c3ra45312j