1-((2S,3S,4S,5S)-5-Bromomethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione

Base Information

• Chemical Name: 1-((2S,3S,4S,5S)-5-Bromomethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione
• CAS No.: 80541-18-0
• Molecular Formula: C₉H₁₁BrN₂O₅
• Molecular Weight: 307.101

Synonyms:1-((2S,3S,4S,5S)-5-Bromomethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione

Chemical Property of 1-((2S,3S,4S,5S)-5-Bromomethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione

Chemical Property:

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Technology Process of 1-((2S,3S,4S,5S)-5-Bromomethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione

There total 1 articles about 1-((2S,3S,4S,5S)-5-Bromomethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

1-(2,5-Anhydro-β-D-arabinofuranosyl)pyrimidin-2,4(1H,3H)-dione (3257-75-8) → 1-((2R,3S,4S,5S)-5-Bromomethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione (59968-05-7) + 1-((2S,3S,4S,5S)-5-Bromomethyl-3,4-dihydroxy-tetrahydro-furan-2-yl)-1H-pyrimidine-2,4-dione (80541-18-0) + uracil (66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6)

Guidance literature:

With hydrogen bromide; In N,N-dimethyl-formamide; at 120 ℃; for 0.0833333h;

Reference yield: 60.0%

5'-bromo-5'-deoxyuridine (19556-55-9,24514-29-2,59968-05-7,80541-18-0) → C8H8N2O5 + 5'-deoxyuridine (15958-99-3)

Guidance literature:

With tri-n-butyl-tin hydride; In benzene; UV-irradiation;

DOI:10.2174/157017811795685108

Reference yield:

5'-bromo-5'-deoxyuridine (19556-55-9,24514-29-2,59968-05-7,80541-18-0) + p-toluenesulfonyl chloride (98-59-9) → 5'-bromo-O2'-(toluene-4-sulfonyl)-5'-deoxy-uridine (130986-49-1)

Guidance literature:

With pyridine;

DOI:10.1093/jat/24.4.271

upstream raw materials:

1-(2,5-Anhydro-β-D-arabinofuranosyl)pyrimidin-2,4(1H,3H)-dione

Downstream raw materials:

5'-bromo-O^2'-(toluene-4-sulfonyl)-5'-deoxy-uridine

5'-deoxyuridine

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