2-Bromo-2-nitroadamantane

Base Information

• Chemical Name: 2-Bromo-2-nitroadamantane
• CAS No.: 40854-02-2
• Molecular Formula: C₁₀H₁₄BrNO₂
• Molecular Weight: 260.131
• Mol file: 40854-02-2.mol

Synonyms:2-bromo-2-nitro-adamantane

Chemical Property of 2-Bromo-2-nitroadamantane

Chemical Property:

Purity/Quality:

2-BROMO-2-NITROADAMANTANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Bromo-2-nitroadamantane

There total 4 articles about 2-Bromo-2-nitroadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-adamantanone oxime (4500-12-3) → 2-bromo-2-nitro-adamantane (40854-02-2)

Guidance literature:

With aluminum oxide; Oxone; potassium bromide; In chloroform; at 45 ℃; for 1h;

DOI:10.1016/S0040-4020(99)00265-3

Reference yield: 50.0%

2-adamantanone oxime (4500-12-3) → 2-Adamantanone (700-58-3) + 2-bromo-2-nitro-adamantane (40854-02-2)

Guidance literature:

With chloroperoxidase from fungus Caldaromyces fumago; dihydrogen peroxide; potassium bromide; In water; for 4h;

DOI:10.1021/jo961215n

Reference yield:

2-bromo-2-nitrosoadamantane → 2-bromo-2-nitro-adamantane (40854-02-2)

Guidance literature:

With nitric acid; In Petroleum ether; for 0.0833333h;

DOI:10.1021/jm00044a010

upstream raw materials:

2-adamantanone oxime

2-Adamantanone

Downstream raw materials:

2-nitroadamantane

2,2-dinitroadamantane