C₅₁H₆₄O₈

Base Information

Chemical Name:C₅₁H₆₄O₈
CAS No.:1449419-28-6
Molecular Formula:C₅₁H₆₄O₈
Molecular Weight:805.064
Hs Code.:

C<sub>51</sub>H<sub>64</sub>O<sub>8</sub>

Synonyms:C₅₁H₆₄O₈

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Chemical Property of C₅₁H₆₄O₈

Chemical Property:

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Technology Process of C₅₁H₆₄O₈

There total 8 articles about C₅₁H₆₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1160697-52-8
C₃₁H₄₂O₄

: 1449419-25-3
C₂₀H₂₄O₅

: 1449419-28-6
C₅₁H₆₄O₈

Guidance literature:: C₂₀H₂₄O₅; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 20 ℃; for 3h;

C₃₁H₄₂O₄; With dmap; In toluene; at 50 ℃; for 1.5h;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-17-3
C₁₅H₂₀O₃S₂

: 1449419-28-6
C₅₁H₆₄O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C

1.2: 2.5 h / 0 - 20 °C

2.1: magnesium bromide ethyl etherate / dichloromethane / 1 h / -78 °C

2.2: 1.5 h / -78 °C

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C

4.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

5.2: 21.5 h / 0 - 20 °C

6.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

7.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

8.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

8.2: 1.5 h / 50 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; di-isopropyl azodicarboxylate; 2,4,6-trichlorobenzoyl chloride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; magnesium bromide ethyl etherate; triethylamine; triphenylphosphine; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 2.2: |Grignard Reaction / 3.1: |Mitsunobu Displacement / 8.1: |Yamaguchi Lactonization / 8.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-19-5
C₁₆H₂₄O₃S₂

: 1449419-28-6
C₅₁H₆₄O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C

2.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 21.5 h / 0 - 20 °C

4.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

5.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

6.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

6.2: 1.5 h / 50 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; di-isopropyl azodicarboxylate; 2,4,6-trichlorobenzoyl chloride; sodium hydride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 1.1: |Mitsunobu Displacement / 6.1: |Yamaguchi Lactonization / 6.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008