C₅₈H₇₃NO₁₈S₂

Base Information

Chemical Name:C₅₈H₇₃NO₁₈S₂
CAS No.:1334524-27-4
Molecular Formula:C₅₈H₇₃NO₁₈S₂
Molecular Weight:1136.35
Hs Code.:

C<sub>58</sub>H<sub>73</sub>NO<sub>18</sub>S<sub>2</sub>

Synonyms:C₅₈H₇₃NO₁₈S₂

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Chemical Property of C₅₈H₇₃NO₁₈S₂

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Technology Process of C₅₈H₇₃NO₁₈S₂

There total 6 articles about C₅₈H₇₃NO₁₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1334524-26-3
C₆₇H₉₃NO₁₈S₂Si

: 1334524-27-4
C₅₈H₇₃NO₁₈S₂

Guidance literature:: With pyridine; hydrogen fluoride; In acetonitrile; at 0 - 20 ℃; for 25h;

Reference yield:

: 452072-22-9
(±)-4-(pyridin-2-yldisulfanyl)pentanoic acid

: 1334524-27-4
C₅₈H₇₃NO₁₈S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 1.5 h / -10 - 20 °C / Inert atmosphere

3.1: diisopropyl-carbodiimide / dichloromethane / 0.17 h / 0 °C

3.2: 5 h / 0 °C

4.1: pyridine hydrogenfluoride / pyridine; acetonitrile / 0 - 20 °C / Inert atmosphere

With pyridine hydrogenfluoride; triethylamine; diisopropyl-carbodiimide; In tetrahydrofuran; pyridine; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.05.039

Reference yield:

: 1334524-24-1
triisopropylsilyl 4-(pyridine-2-yldisulfanyl)pentanoate

: 1334524-27-4
C₅₈H₇₃NO₁₈S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 1.5 h / -10 - 20 °C / Inert atmosphere

2.1: diisopropyl-carbodiimide / dichloromethane / 0.17 h / 0 °C

2.2: 5 h / 0 °C

3.1: pyridine hydrogenfluoride / pyridine; acetonitrile / 0 - 20 °C / Inert atmosphere

With pyridine hydrogenfluoride; diisopropyl-carbodiimide; In tetrahydrofuran; pyridine; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.05.039