1α,5β-Di-(3,4-dimethoxyphenyl)-2β,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

Base Information

• Chemical Name: 1α,5β-Di-(3,4-dimethoxyphenyl)-2β,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene
• CAS No.: 118353-36-9
• Molecular Formula: C₃₃H₄₀O₆
• Molecular Weight: 532.677

Synonyms:1α,5β-Di-(3,4-dimethoxyphenyl)-2β,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

Chemical Property of 1α,5β-Di-(3,4-dimethoxyphenyl)-2β,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

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Technology Process of 1α,5β-Di-(3,4-dimethoxyphenyl)-2β,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

There total 2 articles about 1α,5β-Di-(3,4-dimethoxyphenyl)-2β,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-1,2-Di-(3,4-dimethoxyphenyl)-anti-cis-3,4-dimethylcyclobutane (58045-93-5) → 1,2-dimethoxy-4-(E)-propenylbenzene (6379-72-2) + 1α-(3,4-Dimethoxyphenyl)-2β-methyl-3β-ethyl-5,6-dimethoxyindan (62211-17-0) + 1α,5β-Di-(3,4-dimethoxyphenyl)-2β,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene (118353-36-9) + 1β,5β-Di-(3,4-dimethoxyphenyl)-2α,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene (118353-37-0)

Guidance literature:

With sodium carbonate; tris-(4-bromophenyl)aminium hexachloroantimonate; In dichloromethane; for 15h; Further byproducts given; Ambient temperature;

DOI:10.1021/ja00187a029

Reference yield:

cis-1,2-Di-(3,4-dimethoxyphenyl)-anti-cis-3,4-dimethylcyclobutane (58045-93-5) → 1,2-dimethoxy-4-(E)-propenylbenzene (6379-72-2) + 1α,5β-Di-(3,4-dimethoxyphenyl)-2β,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene (118353-36-9) + 1β,5β-Di-(3,4-dimethoxyphenyl)-2α,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene (118353-37-0) + 1β,5β-Di-(3,4-dimethoxyphenyl)-2α,3α,4α-trimethyl-7,8-dimethoxy-1,2,2a(Hβ),3,4,5-hexahydroacenaphthylene (118353-38-1)

Guidance literature:

With sodium carbonate; tris-(4-bromophenyl)aminium hexachloroantimonate; In dichloromethane; for 15h; Further byproducts given; Ambient temperature;

DOI:10.1021/ja00187a029

upstream raw materials:

cis-1,2-Di-(3,4-dimethoxyphenyl)-anti-cis-3,4-dimethylcyclobutane

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