Technology Process of C33H39IN6O5
There total 12 articles about C33H39IN6O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; N-iodomorpholine-hydrogen iodide;
In
tetrahydrofuran;
at 20 ℃;
Molecular sieve;
DOI:10.1021/ol201567s
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrabutyl ammonium fluoride; sodium hydride / tetrahydrofuran / 20 °C
1.2: 20 °C
2.1: hydrogenchloride / 1,4-dioxane / 20 °C
3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
4.1: copper(l) iodide; N-iodomorpholine-hydrogen iodide / tetrahydrofuran / 20 °C / Molecular sieve
With
hydrogenchloride; copper(l) iodide; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-iodomorpholine-hydrogen iodide; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1021/ol201567s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / 1,4-dioxane / 20 °C
2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
3: copper(l) iodide; N-iodomorpholine-hydrogen iodide / tetrahydrofuran / 20 °C / Molecular sieve
With
hydrogenchloride; copper(l) iodide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-iodomorpholine-hydrogen iodide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1021/ol201567s
