benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate

Base Information

Chemical Name:benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate
CAS No.:828930-60-5
Molecular Formula:C₄₇H₇₁N₂O₂₂P
Molecular Weight:1047.05
Hs Code.:

benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate

Synonyms:benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate

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Chemical Property of benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate

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Technology Process of benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate

There total 9 articles about benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 828930-58-1
3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propylphosphonic acid

: 149359-36-4
benzyl (R)-3-hydroxy-2-octyloxypropanoate

: 828930-60-5
benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate

Guidance literature:: With pyridine; trichloroacetonitrile; at 70 ℃; for 42h;
DOI:10.1016/j.bmc.2004.09.019

Reference yield:

: (R)-3-Hydroxy-2-octyloxy-propionaldehyde

: 828930-60-5
benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 206 mg / silver(I) oxide; sodium hydroxide / tetrahydrofuran; H₂O / 6 h / 20 °C

2: 89 percent / sodium hydrogen carbonate / dimethylformamide / 24 h / 70 °C

3: 79 percent / trichloroacetonitrile; pyridine / 42 h / 70 °C

With pyridine; sodium hydroxide; sodium hydrogencarbonate; trichloroacetonitrile; silver(l) oxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.09.019

Reference yield:

: 828930-52-5
3-bromopropyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranoside

: 828930-60-5
benzyl (R)-3-[3-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyloxy)propyl-hydroxy-phosphinoyloxy]-2-octyloxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 94 percent / 42 h / Heating

2.1: bromotrimethylsilane / CH₂Cl₂ / 2 h

2.2: 100 percent / water / acetone / 0.33 h

3.1: 79 percent / trichloroacetonitrile; pyridine / 42 h / 70 °C

With pyridine; trimethylsilyl bromide; trichloroacetonitrile; In dichloromethane; 1.1: Arbuzov reaction;
DOI:10.1016/j.bmc.2004.09.019