2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide

Base Information

Chemical Name:2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide
CAS No.:1420764-54-0
Molecular Formula:C₂₇H₂₄N₂O₇S
Molecular Weight:520.563
Hs Code.:

Synonyms:2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide

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Chemical Property of 2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide

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Technology Process of 2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide

There total 5 articles about 2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1420764-51-7
2-[(acetylsulfanyl)methyl]-3-(carboxymethoxy)phenoxyacetic acid

: 529-23-7
o-aminobenzaldehyde

: 1420764-54-0
2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide

Guidance literature:: With 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/cssc.201200572

Reference yield:

: 608-25-3
2-methylbenzene-1,3-diol

: 1420764-54-0
2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetone / 2 h / 60 °C / Inert atmosphere

1.2: 48 h / Reflux; Inert atmosphere

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere

3.1: acetone / 20 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

5.1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 20 °C / Inert atmosphere

With N-Bromosuccinimide; 2-chloro-1-methyl-pyridinium iodide; potassium carbonate; triethylamine; trifluoroacetic acid; dibenzoyl peroxide; In tetrachloromethane; dichloromethane; acetone;
DOI:10.1002/cssc.201200572

Reference yield:

: 1420764-35-7
2,6-bis(tert-butoxycarbonylmethoxy)toluene

: 1420764-54-0
2-{2-[(acetylsulfanyl)methyl]-3-{[(2-formylphenyl)carbamoyl]methoxy}phenoxy}-N-(2-formylphenyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere

2: acetone / 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

4: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 20 °C / Inert atmosphere

With N-Bromosuccinimide; 2-chloro-1-methyl-pyridinium iodide; triethylamine; trifluoroacetic acid; dibenzoyl peroxide; In tetrachloromethane; dichloromethane; acetone;
DOI:10.1002/cssc.201200572