Technology Process of C17H19BrO9
There total 12 articles about C17H19BrO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C17H17BrO7;
With
4-methylmorpholine N-oxide;
In
water; acetone;
at 20 ℃;
for 0.0833333h;
With
osmium(VIII) oxide;
In
water; acetone;
at 20 ℃;
for 14h;
DOI:10.1021/ol102848w
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: toluene-4-sulfonic acid / dichloromethane / 0.17 h / 0 °C
2.1: phenyltrimethylammonium tribromide / tetrahydrofuran / 12 h / 20 °C
2.2: 0.17 h / 0 °C
3.1: sodium cyanide; manganese(IV) oxide / 4 h / 0 - 20 °C
4.1: 4-methylmorpholine N-oxide / water; acetone / 0.08 h / 20 °C
4.2: 10 h / 20 °C
5.1: dmap / dichloromethane / 0 - 20 °C / Inert atmosphere
6.1: 4-methylmorpholine N-oxide / water; acetone / 0.08 h / 20 °C
6.2: 14 h / 20 °C
With
dmap; sodium cyanide; manganese(IV) oxide; phenyltrimethylammonium tribromide; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; water; acetone;
1.1: Mukaiyama reaction;
DOI:10.1021/ol102848w
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: pyridine; Lindlar's catalyst; hydrogen / ethyl acetate / 1 h
2.1: toluene-4-sulfonic acid / dichloromethane / 0.17 h / 0 °C
3.1: phenyltrimethylammonium tribromide / tetrahydrofuran / 12 h / 20 °C
3.2: 0.17 h / 0 °C
4.1: sodium cyanide; manganese(IV) oxide / 4 h / 0 - 20 °C
5.1: 4-methylmorpholine N-oxide / water; acetone / 0.08 h / 20 °C
5.2: 10 h / 20 °C
6.1: dmap / dichloromethane / 0 - 20 °C / Inert atmosphere
7.1: 4-methylmorpholine N-oxide / water; acetone / 0.08 h / 20 °C
7.2: 14 h / 20 °C
With
pyridine; dmap; sodium cyanide; manganese(IV) oxide; Lindlar's catalyst; hydrogen; phenyltrimethylammonium tribromide; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; water; ethyl acetate; acetone;
2.1: Mukaiyama reaction;
DOI:10.1021/ol102848w