O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate

Base Information

Chemical Name:O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate
CAS No.:741252-62-0
Molecular Formula:C₃₃H₂₈NO₄P
Molecular Weight:533.563
Hs Code.:

Synonyms:O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate

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Chemical Property of O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate

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Technology Process of O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate

There total 3 articles about O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 67515-49-5
1-benzyloxyallene

: 741252-60-8
O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-allylamidophosphate

: 741252-62-0
O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate

Guidance literature:: With 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate; In acetonitrile; at 60 ℃; for 16h;

Reference yield:

: 124583-86-4,124583-87-5,124648-60-8
(+/-)-1,1'-Binaphthyl-2,2'-diyl phosphorochloridate

: 741252-62-0
O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.30 g / CH₂Cl₂ / 17 h / 0 - 20 °C

2: 89 percent / Et₃N; dppp / Pd(OAc)2 / acetonitrile / 16 h / 60 °C

With 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate; In dichloromethane; acetonitrile;

Reference yield:

: 602-09-5
1,1'-bi-2-naphthol

: 741252-62-0
O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-allylamido phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃; Et₃N / CH₂Cl₂ / 0.5 h

2: 1.30 g / CH₂Cl₂ / 17 h / 0 - 20 °C

3: 89 percent / Et₃N; dppp / Pd(OAc)2 / acetonitrile / 16 h / 60 °C

With 1,3-bis-(diphenylphosphino)propane; triethylamine; trichlorophosphate; palladium diacetate; In dichloromethane; acetonitrile;