{2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate

Base Information

Chemical Name:{2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate
CAS No.:1073557-34-2
Molecular Formula:C₁₉H₃₁NO₆S
Molecular Weight:401.524
Hs Code.:

Synonyms:{2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate

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Chemical Property of {2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate

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Technology Process of {2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate

There total 2 articles about {2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1073557-33-1
N-(2-hydroxyethyl)-4-methoxy-2,3,6,N-tetramethylbenzenesulfonamide

: 1073557-34-2
{2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In toluene; at 20 ℃; for 3.5h;

Reference yield:

: 80745-07-9
4-methoxy-2,3,6-trimethylbenzenesulfonyl chloride

: 1073557-34-2
{2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / 20 °C

2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / toluene / 3.5 h / 20 °C

With tetra(n-butyl)ammonium hydrogensulfate; triethylamine; sodium hydroxide; In dichloromethane; toluene;

Reference yield: 99.0%

: 1073557-34-2
{2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate

: 1073556-99-6
2-[2-[[(4-methoxy-2,3,6-trimethyl-phenyl)sulfonyl]-methyl-amino]-ethoxy]-acetic acid

Guidance literature:: {2-[(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-methylamino]-ethoxy}acetic acid tert-butyl acetate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;

With sodium hydrogencarbonate; In water; ethyl acetate;