(1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate

Base Information

Chemical Name:(1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate
CAS No.:1161147-30-3
Molecular Formula:C₁₅H₁₉BrO₈
Molecular Weight:407.215
Hs Code.:

Synonyms:(1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate

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Technology Process of (1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate

There total 2 articles about (1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1161745-98-7
C₁₅H₂₀O₉

: 1161147-30-3
(1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 - 20 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol9008987

Reference yield:

: 1161745-98-7
C₁₅H₂₀O₉

: 1161147-30-3
(1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate

: 1161147-39-2
(1R,2S,3S,6S)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate

Guidance literature:: With phosphorus tribromide; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol9008987

Reference yield:

: 1161147-30-3
(1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate

: 161596-95-8
(1S,2S,3S,4S)-5-(hydroxymethyl)cyclohex-5-ene-1,2,3,4-tetraol

Guidance literature:: (1R,2S,3S,6R)-4-(acetoxymethyl)-6-bromocyclohex-4-ene-1,2,3-triyl triacetate; With ethanol; silver carbonate; for 48h; Inert atmosphere; Reflux;

With methanol; triethylamine; at 40 ℃; for 15h; Inert atmosphere;
DOI:10.1021/ol9008987