4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

Base Information

• Chemical Name: 4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile
• CAS No.: 38477-34-8
• Molecular Formula: C₁₉H₁₄N₂O₃
• Molecular Weight: 318.332

Synonyms:4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

Chemical Property of 4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

Chemical Property:

Purity/Quality:

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Technology Process of 4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile

There total 2 articles about 4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(E)-3-(benzo[d][1,3]dioxol-5-yl)-1-phenylprop-2-en-1-one (644-34-8,54619-91-9) + cyanoacetic acid amide (107-91-5) → 4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile (38477-34-8)

Guidance literature:

With sodium ethanolate; In ethanol; for 1h; boiling water bath;

Reference yield:

→ 4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile (38477-34-8)

Guidance literature:

Chalcon IIb,Ethylcyanoacetat,Ammoniumacetat;

Reference yield:

4-Benzo[1,3]dioxol-5-yl-2-oxo-6-phenyl-1,2,3,4-tetrahydro-pyridine-3-carbonitrile (38477-34-8) → 4-(benzo[d][1,3]dioxol-5-yl)-2-oxo-6-phenyl-1,2-dihydropyridine-3-carbonitrile (38468-91-6)

Guidance literature:

With selenium; at 160 - 170 ℃; for 1h;

upstream raw materials:

(E)-3-(benzo[d][1,3]dioxol-5-yl)-1-phenylprop-2-en-1-one

cyanoacetic acid amide

Downstream raw materials:

4-(benzo[d][1,3]dioxol-5-yl)-2-oxo-6-phenyl-1,2-dihydropyridine-3-carbonitrile

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