(2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

Base Information

Chemical Name:(2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester
CAS No.:1190397-50-2
Molecular Formula:C₃₂H₅₅NO₅Si₂
Molecular Weight:589.963
Hs Code.:

(2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

Synonyms:(2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

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Chemical Property of (2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

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Technology Process of (2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

There total 1 articles about (2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1190397-49-9
(2R)-2,3-dihydro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4(1H)-pyridinone

: 501-53-1,94274-21-2
benzyl chloroformate

: 1190397-50-2
(2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

Guidance literature:: (2R)-2,3-dihydro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4(1H)-pyridinone; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h;

benzyl chloroformate; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;
DOI:10.1021/jo901481n

Reference yield: 89.0%

: 1190397-50-2
(2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

: 1190397-51-3
(2R,4S)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-4-hydroxy-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-1(2H)-pyridinecarboxylic acid phenylmethyl ester

Guidance literature:: With methanol; sodium tetrahydroborate; cerium(III) chloride heptahydrate; at -40 ℃; for 0.5h;
DOI:10.1021/jo901481n

Reference yield: 61.0%

: 1190397-50-2
(2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

: 1235765-33-9
(2R,4R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-4-hydroxy-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-1(2H)-pyridinecarboxylic acid phenylmethyl ester

Guidance literature:: (2R)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-3,4-dihydro-6-[3-[[tris(1-methylethyl)silyl]oxy]propyl]-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester; With 2,6-di-tert-butyl-4-methyl-phenol; diisobutylaluminium hydride; In toluene; at -40 - 0 ℃;

In toluene; at 0 ℃; for 2h;
DOI:10.1021/jo101010c