Technology Process of C57H77N4O14P
There total 9 articles about C57H77N4O14P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride;
In
pyridine;
at 20 - 45 ℃;
for 2h;
DOI:10.1016/0008-6215(96)00042-0
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / PCl3 / acetonitrile / 0.58 h / 20 °C
2: sym-collidine / tetrahydrofuran / 0.5 h / -78 °C
3: NaHCO3; water / tetrahydrofuran
4: I2; water / tetrahydrofuran; pyridine / 0.25 h
5: 82 percent / 2,4,6-tri-isopropylbenzenesulfonyl chloride; 1-methylimidazole / pyridine / 2 h / 20 - 45 °C
With
1-methyl-1H-imidazole; 2,4,6-trimethyl-pyridine; 2,4,6-triisopropylphenylsulfonyl chloride; water; iodine; sodium hydrogencarbonate; phosphorus trichloride;
In
tetrahydrofuran; pyridine; acetonitrile;
1: phosphorodichloriditation / 2: phosphitylation / 3: Hydrolysis / 4: Oxidation / 5: Esterification;
DOI:10.1016/0008-6215(96)00042-0
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sym-collidine / tetrahydrofuran / 0.5 h / -78 °C
2: NaHCO3; water / tetrahydrofuran
3: I2; water / tetrahydrofuran; pyridine / 0.25 h
4: 82 percent / 2,4,6-tri-isopropylbenzenesulfonyl chloride; 1-methylimidazole / pyridine / 2 h / 20 - 45 °C
With
1-methyl-1H-imidazole; 2,4,6-trimethyl-pyridine; 2,4,6-triisopropylphenylsulfonyl chloride; water; iodine; sodium hydrogencarbonate;
In
tetrahydrofuran; pyridine;
1: phosphitylation / 2: Hydrolysis / 3: Oxidation / 4: Esterification;
DOI:10.1016/0008-6215(96)00042-0
